氫氧化鉀相信大家都不陌生了吧,那么它的質(zhì)量指標(biāo)是什么呢?接下來跟隨小編一起簡單了解一下吧。
Potassium hydroxide is not unfamiliar to everyone, so what is its quality index? Next, follow Xiaobian to have a brief understanding.
1、水不溶物:5%試樣水溶液應(yīng)無色透明。
1. Water insoluble substance: 5% sample solution should be colorless and transparent.
2、鉛:取試樣1g溶于5ml水和11ml稀鹽酸試液的混合液中,冷卻。以此作為試樣液按GT-18方法測定。對照液中的鉛離子量取10μg。
2. Lead: Take 1g sample and dissolve it in a mixture of 5ml water and 11ml dilute hydrochloric acid, then cool it. The sample solution was determined by GT-18 method. The amount of lead ion in the control solution was 10 ug.
3、碳酸鹽:在含量分析中介于酚酞和甲基橙終點(diǎn)之間所耗的每mL 1mol/L硫酸,相當(dāng)于碳酸鉀138、2mg。
3. Carbonate: In content analysis, 1 mol/L sulfuric acid per mL, equivalent to 138 and 2 mg of potassium carbonate, is consumed between the end point of phenolphthalein and methyl orange.
4、重金屬:取試樣670mg,溶于5ml水和5ml稀鹽酸試液(TS-117)的混合液中。加熱至沸,冷卻,用水稀釋至25ml,后過濾。以此作為試樣液,按GT-16方法測定。用含20μg鉛離子的對照液(溶液A)。
4. Heavy metals: sample 670 mg, dissolved in 5 ml water and 5 ml dilute hydrochloric acid test solution (TS-117). Heat to boil, cool, dilute to 25 ml with water, and then filter. The sample solution was determined by GT-16 method. The control solution containing 20 mg lead ion (solution A) was used.
5、汞:按CT-22方法測定。標(biāo)準(zhǔn)液和試樣液按如下方法制備。
5. Mercury: determined by CT-22 method. Standard solution and sample solution are prepared in the following way.
?。?)標(biāo)準(zhǔn)液的制備:按GT-22制各貯液和稀釋液,使所得溶液每ml中含汞1μg。取該溶液1ml,放入-50ml燒杯,加水20ml.1:4稀硫酸溶液1ml和4%高錳酸鉀溶液1ml。用表面皿蓋住燒杯,煮沸數(shù)秒鐘后冷卻,備用。
(1) Preparation of standard solution: According to GT-22, each storage liquid and diluent were prepared, so that the obtained solution contained 1 ug of mercury per ml. Take 1 ml of the solution and put it into a beaker of – 50 ml. Add 20 ml.1:4 dilute sulfuric acid solution 1 ml and 4% potassium permanganate solution 1 ml. Cover the beaker with a surface dish and boil for a few seconds before cooling. Set aside.
?。?)試樣液的制備:取試樣10.0g放入-100ml燒杯,加水15ml使之溶解,加酚酞試液(TS-167)2滴,在不斷攪拌下用1:1稀鹽酸溶液緩慢中和。加1:稀硫酸溶液1ml和4%高錳酸鉀溶液1ml,用表面皿蓋住燒杯,煮沸數(shù)秒鐘后冷卻,備用。
(2) Preparation of sample solution: 10.0 g of sample was put into – 100 ml beaker, 15 ml of water was added to dissolve the sample, 2 drops of TS-167 was added, and 1:1 dilute hydrochloric acid solution was used to neutralize the sample slowly under continuous stirring. Add 1:1 dilute sulfuric acid solution 1 ml and 4% potassium permanganate solution 1 ml. Cover the beaker with a surface dish, boil for a few seconds, then cool down. Set aside.
以上關(guān)于氫氧化鉀的質(zhì)量指標(biāo)就為大家簡單介紹到這里了,如果您還有其它的見解的話,歡迎隨時來電咨詢。
The above quality indicators of potassium hydroxide are briefly introduced here. If you have any other opinions, please feel free to call for advice.